B. Pharmacy 1 year I Semester Pharmaceutical Analysis (PA) Notes as per PCI Syllabus.
B. Pharmacy 1 year I Semester Pharmaceutical Analysis (PA) Notes as per PCI Syllabus.
As the Pharmaceutical Analysis deals with the study of chemical analysis of the drug. The theory paper is of 75 marks + 25 marks internal = 100 marks. As per the PCI criteria for passing is 50% of the total marks including theory paper & internal marks.
The practical exam consist of same criteria as per the theory paper 75/25 pattern. the final practical duration is 3 hrs.
The practical may be consist of
- Major Experiment.
- Minor Experiment.
- Synopsis.
- Viva-voce. (Held by the external examiner conduct as oral)
Pharmaceutical Analysis Unit - I - Chapter - I: Pharmaceutical Analysis.
Definition & scope, Different techniques of analysis, Methods of expressing concentration, primary & secondary standards, preparation of various molar & normal solutions
- Chapter - II: Errors
Sources of errors, types of errors, methods of minimizing errors, accuracy, .precision,& significant figures.
To view the Unit - I notes click on the link PA unit I notes
Unit - II
- Chapter II: Acid base titration
Theories of acid base indicators, classification of acid base titration & theory involved in titrations of strong weak & very weak acids & bases, neutralization curves.
- Chapter III: Non aqueous titrations.
Solvents, acidimetry & alkalimetry titration & estimation of sodium benzoate & ephedrine HCL
To view the Unit - II notes click on the link PA unit II notes
Unit - III
- Chapter IV: Precipitation titrations.
Complexometric titrations: classification, metal ion indicators, masking& demasking reagents, estimation of magnesium sulphate & calcium gluconate.
- Chapter V: Gravimetry.
Unit - IV
- Chapter VI: Redox titrations.
To view the Unit - IV notes click on the link PA unit IV notes
Unit - V
- Chapter VII: Electrochemical methods of Analysis
To view the Unit - V notes click on the link PA unit V notes
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