B. Pharmacy 1 year I Semester Pharmaceutical Analysis (PA) Notes as per PCI Syllabus.

 

  B. Pharmacy 1 year I Semester  Pharmaceutical Analysis (PA) Notes  as per PCI Syllabus.

As the Pharmaceutical Analysis deals with the study of chemical analysis of the drug. The theory paper is of 75 marks + 25 marks internal = 100 marks. As per the PCI criteria for passing is 50% of the total marks including theory paper & internal marks.
The practical exam consist of  same criteria as per the theory paper  75/25 pattern. the final practical duration is 3 hrs.

The practical may be consist of 
  1. Major Experiment.
  2. Minor Experiment. 
  3. Synopsis. 
  4. Viva-voce. (Held by the external examiner conduct as oral)

Pharmaceutical Analysis
   Unit - I 
  • Chapter - I: Pharmaceutical Analysis.
Definition & scope, Different techniques of analysis, Methods of expressing concentration, primary & secondary standards, preparation of various molar & normal solutions

  • Chapter - II: Errors
Sources of errors, types of errors, methods of minimizing errors, accuracy, .precision,& significant figures.



To view the Unit - I notes click on the link    PA unit I notes




Unit - II

  • Chapter II: Acid base titration
Theories of acid base indicators, classification of acid base titration & theory involved in titrations of strong weak & very weak acids & bases, neutralization curves.

  • Chapter III: Non aqueous titrations.
Solvents, acidimetry & alkalimetry titration & estimation of sodium benzoate & ephedrine HCL



To view the Unit - II notes click on the link  PA unit II notes




Unit - III
  • Chapter IV: Precipitation titrations.
Mohr's method, volhard's , modified volhard's, fajan's method,estimation of sodium chloride
Complexometric titrations: classification, metal ion indicators, masking& demasking reagents, estimation of magnesium sulphate & calcium gluconate.

  • Chapter V: Gravimetry.
Principle & steps involved in gravimetric analysis, purity of precipitate: coprecipitation & post precipitations, estimation of barium sulphate



To view the Unit - III notes click on the link  PA unit III notes




Unit - IV 
  • Chapter VI: Redox titrations.


To view the Unit - IV notes click on the link  PA unit IV notes




Unit - V
  • Chapter VII: Electrochemical methods of Analysis


To view the Unit - V notes click on the link   PA unit V notes

 

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